By Oak Ridge National Laboratory. Metallurgy Division.; Union Carbide Corporation
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Phys. Chem. 61, 1131 (1957)28B. R. Sundheim and J. Greenberg, J. Chem. Phys. 28, 439 ( 1 9 5 8 ) . 1. I1 f a c t t h a t they worked a t a path l e n g t h of 2000 p. their A0 h This agrees with t h e Rhodes and U b b e l ~ h d e ~ ~ measured u l t r a v i o l e t s p e c t r a of t h i n films of LiN03, NaNO3, and KNO3 i n both t h e c r y s t a l l i n e and molten s t a t e s . From t h e i r p l o t s t h e coordinates of t h e maximum of band I1 may be estimated f a i r l y w e l l f o r a melt of LiNO3 and r a t h e r roughly f o r a melt of Na;N03.
J. Phys. Chem. 62, 999 (1958). 3T. J. , and D. Cubicciotti, J. Phys. Chem. 62, 843 (1958). ‘T. J. , and D. Cubicciotti, J. Phys. Chem. 63, 1112 (1959). 5T. J. , and D. Cubicciotti, J. Phys. Chem. 63, 1472 (1959). 6S. J. , J. Phys. Chem. 63, 230 (1959). 7M. A. Sokolova, G. G. Urazov, and V. G. Kuznetsov, Khim. Redkikh Elementov, Akad. , Inst. Obshche? i Neorg. Khim. No. 1, p 102 (1954). 8A. H. W. Aten, Z. physik. Chem. 66, 641 (1909). 9D. Cubicciotti and N. L. Lofgren, Trans. Y. Acad. Sei. (in press).
62, 409 ( 1 9 5 8 ) . - 10 s disk into a Pyrex tube, sealed off under vacuum, and later opened in the dry box, where the mete weighing bottle. ingot was broken up in a mortar and placed in a Subsequent handling of bismuth metal was performed in air with minimum exposure time. As an added precaution, the metal was stored in a desiccator. No weight change was detected when bismuth was stored in this way for periods of several months. Measurements. - A Cary model llMS spectrophotometer modified'' for high-temperature work was used to make the spectral measurements.