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Applied pyrolysis handbook by Thomas P. Wampler

By Thomas P. Wampler

"Offers concise insurance of pyrolysis suggestions within the analytical laboratory--concentrating on sensible purposes to real-world samples and pattern kinds. exhibits how pyrolysis can be utilized for quite a lot of fabrics, together with forensic facts, paints, fibers, textiles, paper, ink, photocopies, artwork and museum items, man made polymers, and normal substances."

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If the carrier gas is traveling too slowly through the furnace, the sample may degrade, then have time for the pyrolyzate material to interact with the furnace wall, producing secondary pyrolysis products. In general, reasonable results may be duplicated on the same instrument using the same displayed wall temperature, making the assumption that the internal temperature caused by this wall temperature is also reproduced. 4. Advantages of Furnace Pyrolyzers Because of their simple construction and operation, furnace pyrolyzers are frequently inexpensive and relatively easy to use.

Appl. , 32: 57175726 (1986). 15. C. Hughes, B. B. Wheals, and M. J. Whitehouse, J. Anal. Appl. , 103: 482491 (1978). 16. J. W. Washall and T. P. Wampler, J. Chrom. , 27: 144148 (1989). 17. J. Zimmerman, D. Mooney, and M. J. Kimmet, JFSCA, 31, 2: 489493 (1986). 18. T. P. Wampler and E. J. Levy, LC-GC, 4, 11: 11121116 (1987). 19. A. M. Shedrinsky, T. P. Wampler, and N. S. Baer, The identification of dammar, mastic, sandarac and copals by pyrolysis gas chromatography, Wiener Berichte uber Naturwissenschaft in der Kunst, VWGO, Wien (1988).

Washall and T. P. Wampler, Spectroscopy, 6, 4: 3842 (1991). 13. S. Tsuge, H. Ohtani, T. Nagaya, and Y. Sugimura, J. Anal. Appl. , 4: 117131 (1982). Page 28 14. M. Saglam, J. Appl. , 32: 57175726 (1986). 15. C. Hughes, B. B. Wheals, and M. J. Whitehouse, J. Anal. Appl. , 103: 482491 (1978). 16. J. W. Washall and T. P. Wampler, J. Chrom. , 27: 144148 (1989). 17. J. Zimmerman, D. Mooney, and M. J. Kimmet, JFSCA, 31, 2: 489493 (1986). 18. T. P. Wampler and E. J. Levy, LC-GC, 4, 11: 11121116 (1987).

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